Title: Study on Synthesis of Methyl 4-(bromomethyl)benzoate
Abstract: Methyl 4-(bromomethyl)benzoate was synthesized by the reaction of methyl 4-methylbenzoate with N-bromosuccinimide(NBS).The optimum conditions of synthesizing the compound by orthogonal test obtained were that the molar ratio of N-bromosuccinimide to methyl 4-methylbenzoate was 1.1:1,reaction time was 4 h,the molar ratio of benzoyl peroxide to n-bromosuccinimide was 0.03:1,and the molar ratio of carbon tetrachloride to methyl 4-methylbenzoate was 11:1.Under the optimum synthetic conditions,the yield of the product was 90.5%.
Publication Year: 2012
Publication Date: 2012-01-01
Language: en
Type: article
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