Abstract: One-pot synthesis of N-allylphthalimide from phthalimide and allyl chloride was studied.Effects of feed ratio,reaction temperature,reaction time and solvent were investigated.Best results were obtained under conditions of the molar ratio of allyl chloride to phthalimide of 1.5:1,the temperature of 60℃ and the reaction time of 12 h,and the yield of N-allylphthalimide was 88.5%.The target product was identified with FT-IR and 1H NMR.
Publication Year: 2011
Publication Date: 2011-01-01
Language: en
Type: article
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