Title: Synthesis of Cedryl Acetate under Microwave Irradiation
Abstract: Cedryl acetate was synthesized from cedrol and acetic anhydride by catalysis of mixture of phosphoric acid and acetic acid under microwave irradiation.The optimum reaction condition obtained from orthogonal experiment was as follows: molar ratio of cedrol 5.55g to acetic anhydride 1∶1.5,dosage of catalyst 0.010g,microwave irradiation power 450W and irradiation time 20min.Average yield of cedryl acetate was74.6%.
Publication Year: 2008
Publication Date: 2008-01-01
Language: en
Type: article
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