Title: Synthesis of Ethylimine Acid Ethyl Ester Hydrochloride and Mechanism Investigation
Abstract: Acetonitrile and ethanol as the raw materials to avoid using solvents,ethylimine acid ethyl ester hydrochloride was synthesized.The effects of ratio,temperature,reaction time on the yield of product,and the mechanism of the side-effects of hydrolysis,alcoholysis,and thermal decomposition on the reaction process were analyzed,and the best conditions determined were that reaction molar ratio of acetonitrile to ethanol was 1.3:1,reaction temperature was 35 ℃,and reaction time was 12 h,and the total yield was more than 93%.
Publication Year: 2012
Publication Date: 2012-01-01
Language: en
Type: article
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