Title: Structure Elucidation of Clindamycin Phosphate by NMR Spectroscopy
Abstract: Clindamycin phosphate,an antibiotic drug,was used extensively in clinic.In this study,the 1H,13C and 31P chemical shifts of the compound were assigned using 2D NMR techniques,including DEPT,1H-1H COSY,13C-1H HSQC and 13C-1H HMBC.The relative stereochemistry was established by the results obtained from quantum chemical calculation and NOESY spectroscopy.The fragmentation pathway of clindamycin phosphate was also analyzed by TOF-MS/MS.
Publication Year: 2008
Publication Date: 2008-01-01
Language: en
Type: article
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