Abstract: High performance liquid chromatography(HPLC) method for the determination of acetylacetone was explored.The chromatographic column was Shimadzu VP-ODS(150 mm×4.6 mm,4.6 μm),the mobile phase was methanol(100%),the flow rate was 0.3 mL/min,the UV detection wavelength was 274 nm and the column temperature was 30 °C.Within the range of 15.62~156.2 ng,the content of acetylacetone had a good linear relationship(r=0.999 9),and the average recovery(n=6) was 100.02% with relative standard deviatiom of 1.44%.The method is simple,fast,accurate,and can be used for the content determination of acetylacetone.
Publication Year: 2010
Publication Date: 2010-01-01
Language: en
Type: article
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