Title: Automated Diffraction Tomography for the Structure Elucidation of Twinned, Sub‐micrometer Crystals of a Highly Porous, Catalytically Active Bismuth Metal–Organic Framework
Abstract: Angewandte Chemie International EditionVolume 51, Issue 41 p. 10373-10376 Communication Automated Diffraction Tomography for the Structure Elucidation of Twinned, Sub-micrometer Crystals of a Highly Porous, Catalytically Active Bismuth Metal–Organic Framework† Mark Feyand, Mark Feyand Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany)Search for more papers by this authorDr. Enrico Mugnaioli, Dr. Enrico Mugnaioli Institut für Physikalische Chemie, Johannes Gutenberg-Universität Mainz, Welderweg 11, 55099 Mainz (Germany)Search for more papers by this authorFrederik Vermoortele, Frederik Vermoortele Centre for Surface Chemistry and Catalysis, Kasteelpark Arenberg 23, 3001 Heverlee (Belgium)Search for more papers by this authorBart Bueken, Bart Bueken Centre for Surface Chemistry and Catalysis, Kasteelpark Arenberg 23, 3001 Heverlee (Belgium)Search for more papers by this authorDr. Johannes M. Dieterich, Dr. Johannes M. Dieterich Institut für Physikalische Chemie, Georg-August-Universität Göttingen, Tammannstrasse 6, 37077 Göttingen (Germany)Search for more papers by this authorTim Reimer, Tim Reimer Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany)Search for more papers by this authorDr. Ute Kolb, Corresponding Author Dr. Ute Kolb Institut für Physikalische Chemie, Johannes Gutenberg-Universität Mainz, Welderweg 11, 55099 Mainz (Germany) Ute Kolb, Institut für Physikalische Chemie, Johannes Gutenberg-Universität Mainz, Welderweg 11, 55099 Mainz (Germany) Norbert Stock, Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany)Search for more papers by this authorProf. Dr. Dirk de Vos, Prof. Dr. Dirk de Vos Centre for Surface Chemistry and Catalysis, Kasteelpark Arenberg 23, 3001 Heverlee (Belgium)Search for more papers by this authorProf. Dr. Norbert Stock, Corresponding Author Prof. Dr. Norbert Stock [email protected] Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany) Ute Kolb, Institut für Physikalische Chemie, Johannes Gutenberg-Universität Mainz, Welderweg 11, 55099 Mainz (Germany) Norbert Stock, Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany)Search for more papers by this author Mark Feyand, Mark Feyand Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany)Search for more papers by this authorDr. Enrico Mugnaioli, Dr. Enrico Mugnaioli Institut für Physikalische Chemie, Johannes Gutenberg-Universität Mainz, Welderweg 11, 55099 Mainz (Germany)Search for more papers by this authorFrederik Vermoortele, Frederik Vermoortele Centre for Surface Chemistry and Catalysis, Kasteelpark Arenberg 23, 3001 Heverlee (Belgium)Search for more papers by this authorBart Bueken, Bart Bueken Centre for Surface Chemistry and Catalysis, Kasteelpark Arenberg 23, 3001 Heverlee (Belgium)Search for more papers by this authorDr. Johannes M. Dieterich, Dr. Johannes M. Dieterich Institut für Physikalische Chemie, Georg-August-Universität Göttingen, Tammannstrasse 6, 37077 Göttingen (Germany)Search for more papers by this authorTim Reimer, Tim Reimer Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany)Search for more papers by this authorDr. Ute Kolb, Corresponding Author Dr. Ute Kolb Institut für Physikalische Chemie, Johannes Gutenberg-Universität Mainz, Welderweg 11, 55099 Mainz (Germany) Ute Kolb, Institut für Physikalische Chemie, Johannes Gutenberg-Universität Mainz, Welderweg 11, 55099 Mainz (Germany) Norbert Stock, Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany)Search for more papers by this authorProf. Dr. Dirk de Vos, Prof. Dr. Dirk de Vos Centre for Surface Chemistry and Catalysis, Kasteelpark Arenberg 23, 3001 Heverlee (Belgium)Search for more papers by this authorProf. Dr. Norbert Stock, Corresponding Author Prof. Dr. Norbert Stock [email protected] Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany) Ute Kolb, Institut für Physikalische Chemie, Johannes Gutenberg-Universität Mainz, Welderweg 11, 55099 Mainz (Germany) Norbert Stock, Institut für Anorganische Chemie, Christian Albrechts Universität zu Kiel, Max-Eyth Strasse 2, 24118 Kiel (Germany)Search for more papers by this author First published: 13 September 2012 https://doi.org/10.1002/anie.201204963Citations: 133 † We thank Steffen Schmidt (LMU München) for the SEM micrographs, Michael T. Wharmby for his assistance in preparing the graphics, and the DFG for financial support (SPP 1362, grant agreement no. STO 643/5-2). This work has also been supported by the Stiftung Rheinland-Pfalz für Innovation and the state Schleswig Holstein. Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinkedInRedditWechat Graphical Abstract A combined approach: A permanent highly porous bismuth-containing metal–organic framework (CAU-7) has been synthesized and its structure determined by a combination of electron diffraction, Rietveld refinement, and DFT calculations. The compound is catalytically active in the hydroxymethylation of furan (see picture). Citing Literature Supporting Information Detailed facts of importance to specialist readers are published as ”Supporting Information”. Such documents are peer-reviewed, but not copy-edited or typeset. They are made available as submitted by the authors. Filename Description anie_201204963_sm_miscellaneous_information.pdf10.6 MB miscellaneous_information Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article. Volume51, Issue41October 8, 2012Pages 10373-10376 RelatedInformation
Publication Year: 2012
Publication Date: 2012-09-13
Language: en
Type: article
Indexed In: ['crossref', 'pubmed']
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Cited By Count: 91
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