Title: Solid‐State Protein‐Structure Determination with Proton‐Detected Triple‐Resonance 3D Magic‐Angle‐Spinning NMR Spectroscopy
Abstract: Angewandte ChemieVolume 119, Issue 44 p. 8532-8535 Zuschrift Solid-State Protein-Structure Determination with Proton-Detected Triple-Resonance 3D Magic-Angle-Spinning NMR Spectroscopy† Donghua H. Zhou Dr., Donghua H. Zhou Dr. Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorJohn J. Shea, John J. Shea Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorAndrew J. Nieuwkoop, Andrew J. Nieuwkoop Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorW. Trent Franks, W. Trent Franks Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorBenjamin J. Wylie, Benjamin J. Wylie Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorCharles Mullen, Charles Mullen Varian, Inc. Fort Collins, CO, USASearch for more papers by this authorDennis Sandoz, Dennis Sandoz Varian, Inc. Palo Alto, CA, USASearch for more papers by this authorChad M. Rienstra Prof. Dr., Chad M. Rienstra Prof. Dr. [email protected] Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this author Donghua H. Zhou Dr., Donghua H. Zhou Dr. Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorJohn J. Shea, John J. Shea Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorAndrew J. Nieuwkoop, Andrew J. Nieuwkoop Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorW. Trent Franks, W. Trent Franks Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorBenjamin J. Wylie, Benjamin J. Wylie Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this authorCharles Mullen, Charles Mullen Varian, Inc. Fort Collins, CO, USASearch for more papers by this authorDennis Sandoz, Dennis Sandoz Varian, Inc. Palo Alto, CA, USASearch for more papers by this authorChad M. Rienstra Prof. Dr., Chad M. Rienstra Prof. Dr. [email protected] Department of Chemistry, University of Illinois at Urbana-Champaign, Urbana, IL 61801, USA, Fax: (+1) 217-244-4655 http://www.scs.uiuc.edu/∼rienstraSearch for more papers by this author First published: 02 November 2007 https://doi.org/10.1002/ange.200702905Citations: 28 † This research was supported by the National Institutes of Health (R01 GM-75937 to C.M.R). We thank Philippe Nadaud and Prof. Christopher Jaroniec (Ohio State University) for advice regarding expression of deuterated GB1, and Mircea Cormos and John A. Stringer (Varian, Inc.) for advice on probe performance. Read the full textAboutPDF ToolsRequest permissionAdd to favorites ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinkedInRedditWechat Graphical Abstract Magische Methoden: Die Kombination von schneller Drehung im magischen Winkel, Isotopenverdünnung und hoher Magnetfeldstärke ergibt gut aufgelöste Festkörper-1H-NMR-Spektren, die effizient eingesetzt wurden, um Proteinstrukturen zu lösen. Mit den neuen Techniken genügen nun drei Tage für die Datensammlung, die Zuordnung der Signale zu den Protonen und die Erstellung einer hochaufgelösten Struktur von mikrokristallinem GB1. Citing Literature Supporting Information Supporting information for this article is available on the WWW under http://www.wiley-vch.de/contents/jc_2001/2007/z702905_s.pdf or from the author. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article. Volume119, Issue44November 12, 2007Pages 8532-8535 This is the German version of Angewandte Chemie. Note for articles published since 1962: Do not cite this version alone. Take me to the International Edition version with citable page numbers, DOI, and citation export. We apologize for the inconvenience. RelatedInformation
Publication Year: 2007
Publication Date: 2007-10-01
Language: en
Type: article
Indexed In: ['crossref']
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Cited By Count: 35
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