Title: Study on the Microwave-assisted Benzoin Synthesis with Orthogonal Design
Abstract:The synthesis of benzoin under the condition of microwave-assisted heating was studied.The influence of microwave heating power,microwave heating time,reaction system temperature,and the catalysis dos...The synthesis of benzoin under the condition of microwave-assisted heating was studied.The influence of microwave heating power,microwave heating time,reaction system temperature,and the catalysis dosage on yield were investigated.The results indicate that the influence of the catalysis dosage,reaction system temperature,microwave heating time and microwave heating power on yield decreased in turn and the optimum reaction conditions were the catalysis dosage 1g,reaction system temperature 80℃,microwave heating time 20min and microwave heating power 900W.The melting point and infrared spectrum accord with standard sample.Read More
Publication Year: 2008
Publication Date: 2008-01-01
Language: en
Type: article
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