Abstract: Tribenzyl phosphite is synthesized with phosphorus trichloride and benzyl alcohol as starting materials,N,N-dimethyl aniline as acid binding agent and petroleum ether as solvent.The effects of solvent,reaction temperature and time are discussed in details.The results show that,with(60~90℃)petroleum ether as solvent,dropping temperature 5~10 ℃,reaction temperature 40~50 ℃,reaction time 1 h,the yield of tribenzyl phosphite can be up to 80.5%.
Publication Year: 2006
Publication Date: 2006-01-01
Language: en
Type: article
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