Title: Getermination of Acetone、Acetonitrile、Dichloromethane and Tetrahydrofuran in Biapenem by GC
Abstract: A GC method was established for the determination of Acetone、Acetonitrile、Dichloromethane and Tetrahydrofuran in Biapenem.The fixed phase(6%),cyanide phenyl propyl-(94%),dimethyl polysiloxane capillary column Temperrature of oven at 50℃,carrier: nitrogen,FID detector at 250℃,Injector at 200℃,The calibration curves of Acetone、Acetonitrile、Dichloromethane and Tetrahydrofuran were linear in the concentration ranges of 0.1~0.6mg/mL、0.0082~0.0492mg/mL、0.12~0.072mg/mL and 0.0144~ 0.0864mg/mL.The recoveries of Acetone、Acetonitrile、Dichloromethane and Tetrahydrofuran were106.25%、110.19%、99.16%、 101.43%.The RSD of were 0.28%、3.43%、2.57%、1.59%.
Publication Year: 2010
Publication Date: 2010-01-01
Language: en
Type: article
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