Title: Determination of Naringin in Xiqigushang Tablet by HPLC
Abstract: OBJECTIVE To establish an HPLC method for content determination of naringin in Xiqigushang tablet.METHODS The assay was performed on Phenomenex Luna C18 column(250 mm×4.6 mm,5 μm) by UV detector at 283 nm with acetonitrile-0.05% glacial acetic acid(20∶80) as the mobile phase at the flow rate of 1.0 mL·min 1,column temperature at 30 ℃.RESULTS The amount of naringin was linear with its area over the range of 0.123 0 1.025 2 μg(r=0.999 7),the average recovery and relative standard deviation of naringin were 98.6%,RSD=0.90%(n=6).CONCLUSION The method is sensitive,accurate and can be used for the quality control of Xiqigushang tablet.
Publication Year: 2012
Publication Date: 2012-01-01
Language: en
Type: article
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