Abstract: The objective of this Phase 1 SBIR was to develop and test a long life ZnO-TiO{sub 2} sorbent for hot gas cleanup. Specifically, the authors measured the sulfur loading at space velocities typically used for absorption of H{sub 2}S and regenerated the sorbent with diluted air containing SO{sub 2} for multiple cycles. Based on the experimental results, they prepare a conceptual design of the sorbent fabrication system, and estimated the cost of producing the sorbent and the cost of sulfur removal. Results are presented on tests of sorbents identified as TMZ-6 and TMZ-6II.