Hydrothermal Synthesis of Bi6S2O15 Nanowires: Structural, in situ EXAFS, and Humidity‐Sensing Studies

Name: Hydrothermal Synthesis of Bi6S2O15 Nanowires: Structural, in situ EXAFS, and Humidity‐Sensing Studies
Uploaded: 2010-05-20

Ying Zhou; Jan‐Dierk Grunwaldt; Frank Krumeich; Kaibo Zheng; Guorong Chen; Jan Stötzel; R. Frahm; Greta R. Patzke

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ID: W2069395714
Title: Hydrothermal Synthesis of Bi6S2O15 Nanowires: Structural, in situ EXAFS, and Humidity‐Sensing Studies
Abstract: SmallVolume 6, Issue 11 p. 1173-1179 Communication Hydrothermal Synthesis of Bi6S2O15 Nanowires: Structural, in situ EXAFS, and Humidity-Sensing Studies† Ying Zhou, Ying Zhou Institute of Inorganic Chemistry, University of Zurich Winterthurerstr. 190, 8057 Zurich (Switzerland)Search for more papers by this authorJan-Dierk Grunwaldt, Jan-Dierk Grunwaldt Department of Chemical and Biochemical Engineering Technical University of Denmark 2800 Kgs. Lyngby (Denmark) Institute for Chemical Technology and Polymer Chemistry Karlsruhe Institute of Technology (KIT) 76128 Karlsruhe (Germany)Search for more papers by this authorFrank Krumeich, Frank Krumeich Laboratory of Inorganic Chemistry ETH Zurich 8093 Zurich (Switzerland)Search for more papers by this authorKaibo Zheng, Kaibo Zheng Department of Materials Science Fudan University 220 Handan Road, 200433 Shanghai (P. R. China)Search for more papers by this authorGuorong Chen, Guorong Chen Department of Materials Science Fudan University 220 Handan Road, 200433 Shanghai (P. R. China)Search for more papers by this authorJan Stötzel, Jan Stötzel Department of Physics, University of Wuppertal 42097 Wuppertal (Germany)Search for more papers by this authorRonald Frahm, Ronald Frahm Department of Physics, University of Wuppertal 42097 Wuppertal (Germany)Search for more papers by this authorGreta R. Patzke, Corresponding Author Greta R. Patzke [email protected] Institute of Inorganic Chemistry, University of Zurich Winterthurerstr. 190, 8057 Zurich (Switzerland)Institute of Inorganic Chemistry, University of Zurich Winterthurerstr. 190, 8057 Zurich (Switzerland)Search for more papers by this author Ying Zhou, Ying Zhou Institute of Inorganic Chemistry, University of Zurich Winterthurerstr. 190, 8057 Zurich (Switzerland)Search for more papers by this authorJan-Dierk Grunwaldt, Jan-Dierk Grunwaldt Department of Chemical and Biochemical Engineering Technical University of Denmark 2800 Kgs. Lyngby (Denmark) Institute for Chemical Technology and Polymer Chemistry Karlsruhe Institute of Technology (KIT) 76128 Karlsruhe (Germany)Search for more papers by this authorFrank Krumeich, Frank Krumeich Laboratory of Inorganic Chemistry ETH Zurich 8093 Zurich (Switzerland)Search for more papers by this authorKaibo Zheng, Kaibo Zheng Department of Materials Science Fudan University 220 Handan Road, 200433 Shanghai (P. R. China)Search for more papers by this authorGuorong Chen, Guorong Chen Department of Materials Science Fudan University 220 Handan Road, 200433 Shanghai (P. R. China)Search for more papers by this authorJan Stötzel, Jan Stötzel Department of Physics, University of Wuppertal 42097 Wuppertal (Germany)Search for more papers by this authorRonald Frahm, Ronald Frahm Department of Physics, University of Wuppertal 42097 Wuppertal (Germany)Search for more papers by this authorGreta R. Patzke, Corresponding Author Greta R. Patzke [email protected] Institute of Inorganic Chemistry, University of Zurich Winterthurerstr. 190, 8057 Zurich (Switzerland)Institute of Inorganic Chemistry, University of Zurich Winterthurerstr. 190, 8057 Zurich (Switzerland)Search for more papers by this author First published: 31 May 2010 https://doi.org/10.1002/smll.201000112Citations: 26 † We gratefully acknowledge the Swiss Light Source (SLS, Villigen, Switzerland) for providing beam time at the superXAS beamline for QEXAFS experiments. We are grateful to M. J. Beier for help and J.D.G. to DANSCATT for financial support. The support of the Electron Microscopy ETH Zurich, EMEZ, and Center for Microscopy and Image Analysis, University of Zurich, is acknowledged. We are grateful to Prof. W. Bensch and Dr. N. Pienack (University of Kiel, Germany) for in situ EDXRD experiments and to HASYLAB (DESY, Hamburg, Germany) for providing beam time at beamline F3. Financial support from the Sino Swiss Science and Technology Cooperation (SSSTC, project no. EG05-092008) is gratefully acknowledged. We thank the Swiss National Science Foundation (SNF Professorship PP002 - 114711/1) and the University of Zurich for financial support. Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onEmailFacebookTwitterLinkedInRedditWechat Graphical Abstract Sensing oxysulfates: A new type of bismuth oxysulfate nanowire emerges from the straightforward hydrothermal reaction of Bi2O3 and K2SO4. The formation pathway of this versatile material is monitored with in situ QEXAFS techniques. The high-aspect-ratio nanorods display promising features for application in humidity sensors. Supporting Information Detailed facts of importance to specialist readers are published as ”Supporting Information”. Such documents are peer-reviewed, but not copy-edited or typeset. They are made available as submitted by the authors. Filename Description smll_201000112_sm_suppdata.pdf856.3 KB suppdata Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article. References 1a C. N. R. Rao, F. L. Deepak, G. Gundiah, A. Govindaraj, Prog. Solid State Chem. 2005, 31, 5; 1b G. R. Patzke, F. Krumeich, R. Nesper, Angew. Chem. Int. Ed. 2003, 42, 972. 2a G. Shen, P. Chen, K. Ryu, C. Zhou, J. Mater. Chem. 2009, 19, 828; 2b Y. Xia, P. 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Publication Year: 2010
Publication Date: 2010-05-20
Language: en
Type: article
Indexed In: ['crossref', 'pubmed']

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1395, 1429, 1448, 1471, 1494, 1590, 1614, 1639], '2005,': [759, 1044, 1111, 1128, 1140, 1371], '31,': [760], '5;': [761], '1b': [762], 'Nesper,': [769, 1443], 'Angew.': [770, 1024, 1070], 'Int.': [772, 1026, 1072], 'Ed.': [773, 1027, 1073], '2003,': [774, 813, 1259, 1473], '42,': [775, 1411], '972.': [776], '2a': [777], 'Shen,': [779], 'P.': [780, 795, 1001, 1183, 1285, 1657], 'K.': [782, 860, 985, 1003, 1174, 1501], 'Ryu,': [783], 'Mater.': [787, 812, 863, 889, 916, 937, 954, 991, 1057, 1227, 1238, 1449, 1523, 1546, 1561, 1572], '2009,': [789, 904, 1085, 1280, 1324, 1397, 1524, 1547, 1616], '19,': [790, 939, 1525, 1548], '828;': [791], '2b': [792], 'Y.': [793, 797, 799, 805, 846, 848, 883, 894, 1081, 1454, 1480, 1483, 1566, 1599, 1601, 1635], 'Xia,': [794], 'Yang,': [796, 1490, 1533, 1543, 1569], 'Sun,': [798], 'Wu,': [800, 850, 1080], 'B.': [801, 803, 1019, 1021, 1022, 1143, 1363, 1379, 1385, 1401, 1422, 1485, 1519], 'Mayers,': [802], 'Gates,': [804], 'Yin,': [806], 'Kim,': [808, 1598, 1606], 'H.': [809, 840, 845, 996, 1009, 1404, 1460, 1467, 1597, 1604, 1608, 1622, 1628], 'Yan,': [810, 841], 'Adv.': [811, 1408, 1521, 1544, 1560, 1570], '15,': [814], '353;': [815], '2c': [816], 'Fernandez-Garcia,': [818], 'Martinez-Arias,': [820], 'Hanson,': [823], 'Rodriguez,': [826], 'Rev.': [828, 1330, 1350], '2004,': [829, 917, 1240, 1450], '104,': [830], '4063;': [831], '2d': [832], 'S.': [834, 931, 1007, 1018, 1062, 1121, 1136, 1161, 1263, 1297, 1299, 1402, 1420, 1423, 1489, 1534, 1542, 1568, 1605, 1607], 'Li,': [835, 1504, 1621], 'X.': [836, 1551], 'Long,': [838], 'Nan,': [844], 'Power': [852], 'Sources': [853], '2006,': [854, 955, 1214, 1497], '158,': [855], '1096.': [856], '3': [857], 'Yoshimura,': [859], 'Byrappa,': [861], 'Sci.': [864, 1127, 1331, 1351], '2008,': [865, 890, 1156, 1179, 1353, 1562, 1641], '43,': [866], '2085.': [867], '4a': [868], 'Kiebach,': [870, 924, 943, 1033], 'Pienack,': [872, 897, 945], 'Bensch,': [874, 899, 926, 952, 1039, 1055], 'J.-D.': 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'2269;': [994], '5e': [995], 'Jensen,': [997], 'Bremholm,': [999], 'Nielsen,': [1002], 'Joensen,': [1005], 'Pedersen,': [1008], 'Birkedal,': [1010], 'Y.-S.': [1011], 'Almer,': [1014], 'Søgaard,': [1017], 'Iversen,': [1020, 1023], '46,': [1029, 1075], '1113;': [1030], '5f': [1031], 'Schaefer,': [1035, 1051], 'Porsch,': [1037], 'Z.': [1040, 1079, 1477, 1532, 1581, 1584, 1620], 'Anorg.': [1041], 'Allg.': [1042], '631,': [1045], '369;': [1046], '5g': [1047], 'Engelke,': [1049], 'Schur,': [1053], '2001,': [1058, 1431], '13,': [1059], '1383;': [1060], '5h': [1061], 'Pelster,': [1063], 'Kalamajka,': [1065], 'Schrader,': [1067], 'Schüth,': [1069], '2299.': [1076], '6': [1077], 'Xie,': [1082, 1585], '5943.': [1086], '7a': [1087], 'Vannier,': [1090], 'Mairesse,': [1092], 'Abraham,': [1094], 'Nowogrocki,': [1096], '1996,': [1101, 1196], '122,': [1102], '394;': [1103], '7b': [1104], 'Yu,': [1106, 1466, 1559], 'Kudo,': [1108], 'Lett.': [1110, 1155], '34,': [1112], '1528;': [1113], '7c': [1114], 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'13b': [1336], 'Luetzenkirchen-Hecht,': [1340, 1358, 1388, 1417], 'Fonda,': [1342], 'De': [1344], 'Oliveira,': [1345], 'Briois,': [1347], '79,': [1354], '083107;': [1355], '13c': [1356], 'Richwin,': [1362, 1419], 'Griesebock,': [1364, 1386], 'Physica': [1369], 'Scr.': [1370], 'T115,': [1372], '831;': [1373], '13d': [1374], 'Beier,': [1378], 'Kimmerle,': [1380], 'Nachtegaal,': [1384], '11,': [1398], '8779.': [1399], '14a': [1400], 'Clausen,': [1403, 1424], 'Topsøe,': [1405], '315;': [1412], '14b': [1413], 'Grundmann,': [1421], 'B': [1430], '105,': [1432], '5161.': [1433], '15a': [1434], '1126;': [1452], '15b': [1453], 'Fang,': [1455], 'Xu,': [1457, 1529], 'Song,': [1459], 'Zhang,': [1461, 1531, 1556, 1623], 'You,': [1463], 'Liu,': [1468], '125,': [1474], '16025.': [1475], '16': [1476], 'Gu,': [1479], 'Ma,': [1481], 'Zhai,': [1484], 'Yao,': [1493], 'Eur.': [1495], '12,': [1498], '7717.': [1499], '17a': [1500], 'Xiao,': [1502], 'Tao,': [1506], 'Payzant,': [1509], 'Ivanov,': [1512], 'Puretzky,': [1515], 'Hu,': [1517, 1552], 'Geohegan,': [1520], 'Funct.': [1522, 1545, 1571], '3776;': [1526], '17b': [1527], 'Ding,': [1535], 'Zeng,': [1537], 'Wang,': [1541, 1583, 1627, 1631], '1759.': [1549], '18a': [1550], 'Gong,': [1554], '4845;': [1564], '18b': [1565], 'Qiu,': [1567], '17,': [1574], '1345.': [1575], '19': [1576], 'Kuang,': [1578], 'Lao,': [1580], '129,': [1593], '6070.': [1594], '20': [1595], 'Myung,': [1600], 'Cho,': [1603], 'Park,': [1609, 1611], 'C': [1615], '113,': [1617], '7085.': [1618], '21': [1619], 'Huang,': [1629], 'MacDiarmid,': [1634], 'Wei,': [1636], '130,': [1642], '5036.': [1643], '22Part': [1644], 'Accelrys': [1647, 1652], 'Studio': [1649], 'software': [1650], 'package,': [1651], 'Software': [1653], 'Inc,': [1654], '2001-2009.': [1655], '23': [1656], 'Stadelmann,': [1658], '1987,': [1660], '21,': [1661], '131.': [1662], '24': [1663], 'Ressler,': [1665], 'Synchrotron': [1667], 'Radiat.': [1668], '118.': [1671], 'Citing': [1672], 'Literature': 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