Title: A Sonochemical‐Assisted Synthesis of Pure Nanocrystalline Tetragonal Zirconium Dioxide Using Tetramethylethylenediamine
Abstract:Pure nanocrystalline zirconia has been successfully synthesized by sonochemical‐assisted route from zirconyl nitrate and tetramethylethylenediamine ( TMED ) as starting materials. Here, TMED for the f...Pure nanocrystalline zirconia has been successfully synthesized by sonochemical‐assisted route from zirconyl nitrate and tetramethylethylenediamine ( TMED ) as starting materials. Here, TMED for the first time was used as precipitating agent to generate nanocrystalline tetragonal zirconia via a sonochemical‐assisted route. The effect of solvent and concentration of TMED on the morphology and crystallite size was studied. It was found that these parameters have significant influence on the morphology and crystallite size of the products. The products were characterized by SEM , UV –vis absorption and TEM images, XRD patterns, PL , FTIR , and EDS spectroscopy.Read More
Publication Year: 2014
Publication Date: 2014-05-20
Language: en
Type: article
Indexed In: ['crossref']
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Cited By Count: 46
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