Title: Preparation of bis‐/2‐chloroethyl‐1,2‐<sup>3</sup>H/methylamine hydrochloride
Abstract: Abstract Bis‐(2‐chloroethyl‐1,2‐ 3 H) methylamine hydrochloride was prepared. The starting product was acetylene‐1,2‐ 3 H which was selectively hydrogenated to ethylene‐1,2‐ 3 H. It was observed that on reduction with chromium (II) chloride solution in dilute hydrochloric acid the isotopic exchange with acetylene‐1,2‐ 3 H is negligible. Ethylene was converted to ethyleneoxide‐1,2‐ 3 H by the usual method. Ethyleneoxide‐1,2‐ 3 H can be used for synthesis of several labelled halogenalkylamines and as the starting compound for other syntheses.
Publication Year: 1966
Publication Date: 1966-07-01
Language: en
Type: article
Indexed In: ['crossref']
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